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茶叶中钙元素含量的测定

目录

1 引言.........................................................1 内容来自www.paper51.com

2 实验部分.....................................................1 paper51.com

  2.1火焰原子吸收分光光度法....................................1 paper51.com

    2.1.1实验原理..............................................1

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2.1.2茶叶样品..............................................2 http://www.paper51.com

    2.1.3仪器与试剂............................................2 http://www.paper51.com

2.1.3.1仪器:............................................2

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      2.1.3.2试剂:............................................2 http://www.paper51.com

2.1.3.3仪器工作条件(表1)..............................2 http://www.paper51.com

2.1.4实验步骤..............................................2

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2.1.4.1试样的处理........................................2 内容来自论文无忧网 www.paper51.com

      2.1.4.2标准曲线的绘制....................................3

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2.1.4.2.1  1.000 g/L钙标准贮备液的配置....................3

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2.1.4.2.2  0.0100g/L钙标准使用液的配置....................3 paper51.com

2.1.4.2.3  钙标准曲线的绘制...............................3 paper51.com

2.1.4.2.4  空白样品的配置.................................3

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    2.1.5样品的测定............................................3

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    2.1.6 浸泡法................................................3

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2.2  EDTA滴定法...............................................3 paper51.com

2.2.1 实验原理..............................................3

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2.2.2 茶叶样品..............................................4 paper51.com

2.2.3仪器与试剂.............................................4

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      2.2.3.1仪器:.............................................4 内容来自论文无忧网 www.paper51.com

2.2.3.2试剂:.............................................4 内容来自论文无忧网 www.paper51.com

2.2.4实验步骤..................................................4

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2.2.4.1  0.01mol/LEDTA溶液的配置.............................4

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2.2.4.2以碳酸钙为基准物标定EDTA.............................4 http://www.paper51.com

2.2.4.2.1  配制0.010mol/L钙标准溶液.......................4 paper51.com

2.2.4.2.2  EDTA溶液浓度的标定..............................5 http://www.paper51.com

2.2.4.3 试液中钙离子浓度的测定..............................5 copyright paper51.com

3  实验结果与分析..................................................5

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3.1 火焰原子吸收分光光度法实验结果...............................5

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3.1.1标准曲线的数据...........................................5

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3.1.2 钙标准曲线(图1)........................................6

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3.1.3钙含量测试结果............................................6

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3.1.4 回收率实验................................................7 copyright paper51.com

3.1.5 灰化法测定结果............................................7

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3.1.6 浸泡法测定结果............................................7 http://www.paper51.com

3.2  EDTA滴定法实验结果..........................................8 paper51.com

3.2.1  EDTA溶液浓度的标定......................................8 内容来自www.paper51.com

3.2.2  EDTA滴定法测定试液中钙离子浓度..........................8

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3.3 结果分析......................................................9 内容来自www.paper51.com

4  实验收获.........................................................9

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4.1  能力收获.....................................................9 paper51.com

4.2  知识收获.....................................................9 内容来自www.paper51.com

致谢................................................................9 内容来自www.paper51.com

参考文献...........................................................10

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英文翻译...........................................................11

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